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Nickel-mediated radioiodination of aryl and heteroaryl bromides: rapid synthesis of tracers for SPECT imaging

Author(s): A. A. Cant, S. Champion, R. Bhalla, S. L. Pimlott, A. Sutherland

Rapid and efficient radioiodination of aryl and heteroaryl bromides has been achieved using a nickel(0)-mediated halogen-exchange reaction. This transformation gives direct access to [(123)I]- and [(125)I]-imaging agents for single photon emission computed tomography (SPECT), such as 5-[(123)I]-A85380 (see scheme, Boc = tert-butyloxycarbonyl, cod = 1,5-cyclooctadiene, TFA = trifluoroacetic acid).

Full version: Available here

Click the link to go to an external website with the full version of the paper

ISBN: 1521-3773 (Electronic) 1433-7851 (Linking)
Publication Year: 2013
Periodical: Angew Chem Int Ed Engl
Periodical Number: 30
Volume: 52
Pages: 7829-32
Author Address: WestCHEM, School of Chemistry, University of Glasgow, G12 8QQ, Glasgow, UK.